建立了同时测定配制酒中6种常见芳香物质(苯甲醇、β-苯乙醇、苯甲醛、苯乙酮、丁香醛、肉桂醛)的高效液相色谱法。样品稀释后,用HLB固相柱萃取净化,甲醇洗脱。采用Zobax SB-C18色谱柱(4.6 mm×150 mm,5.0μm),以甲醇和水作为流动相,梯度洗脱。在1.0~20.0 mg/L质量浓度范围内线性相关良好,线性相关系数R2大于0.9998。各组分回收率在87.0%~105.6%之间,相对标准偏差为0.3%~2.1%。 A high performance liquid chromatography (HPLC) was developed for simultaneous determination of six common aromatic compounds (benzyl alcohol, β-phenylethyl alcohol, benzaldehyde, acetophenone, syringaldehyde and cinnamaldehyde) Samples were diluted and purified by HLB solid phase extraction eluting with methanol. A Zobax SB-C18 column (4.6 mm × 150 mm, 5.0 μm) was used with gradient elution with methanol and water as mobile phases. Linear correlation was good in the concentration range of 1.0 ~ 20.0 mg / L, and the linear correlation coefficient R2 was greater than 0.9998. The recoveries of the components ranged from 87.0% to 105.6% with relative standard deviations of 0.3% ~ 2.1%.