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介绍了由CH3SiHCl2和CH3OH进行酯化反应,采用混合溶剂法制备甲基二甲氧基硅[CH3(OCH3)2SiH],研究了不同溶剂和反应条件对醇解反应的影响,对反应产物进行GC—MS,IR定性定量分析,同时确定了较优的合成条件。
The esterification reaction of CH3SiHCl2 and CH3OH was introduced. Methyldimethoxysilane [CH3 (OCH3) 2SiH] was prepared by a mixed solvent method. The effects of different solvents and reaction conditions on the alcoholysis reaction were studied. The reaction products were analyzed by GC -MS, IR qualitative and quantitative analysis, at the same time to determine the better synthesis conditions.