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The title compound,(3R,4R)-4,7,7-trimethyl-6-oxabicyclo[3.2.1]octane-3,4-diol(C10H18O3),has been synthesized by using one-step catalytic synthetic method from a-pinene and structurally characterized by means of IR,~1H-NMR,13C-NMR,HRMS and single-crystal X