Synthesis and Crystal Structure of 9-(4-Methoxylphenyl)-1,8-dioxo-3,4,5,6,7,9-hexahydroxanthene unde

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The crystal structure of the title compound (C20H20O4, Mr = 324.36) has been determined by single-crystal X-ray diffraction. The crystal is of orthorhombic, space group Pbcn with a = 15.823(2), b = 18.002(3), c = 11.674(2) ?, V = 3325.34(67) ?3, Dc = 1.296 g/cm3, μ = 0.090 mm-1, Z = 8, F(000) = 1376, the final R = 0.0421 and wR = 0.0996. In the molecular structure, the pyran ring is of boat conformation, and the two six-membered rings fused with it adopt twisting-boat conformations. The crystal structure of the title compound (C20H20O4, Mr = 324.36) has been determined by single-crystal X-ray diffraction. The crystal is of orthorhombic, space group Pbcn with a = 15.823 (2), b = 18.002 the final R = 0.0421 and wR = (2), V = 3325.34 (67) 3, Dc = 1.296 g / cm3, μ = 0.090 mm-1, Z = 8, F 0.0996. In the molecular structure, the pyran ring is of boat conformation, and the two six-membered rings fused with it adopt twisting-boat conformations.
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