【摘 要】
：
采用电化学方法合成了掺杂聚吡咯钨磷钴和钨磷镍三元杂多酸 ,制备过程简便快速 ,两种混杂有机无机复合物通过电沉积的方法在导电基体玻碳电极上形成膜电极 ,或直接在多酸与吡
【机 构】
：
湖北大学化学与材料科学学院!武汉430062,湖北大学化学与材料科学学院!武汉430062,武汉大学化学与环境科学学院!武汉,武汉大学化学与环境科学学院!武汉
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采用电化学方法合成了掺杂聚吡咯钨磷钴和钨磷镍三元杂多酸 ,制备过程简便快速 ,两种混杂有机无机复合物通过电沉积的方法在导电基体玻碳电极上形成膜电极 ,或直接在多酸与吡咯的硫酸水溶液中电聚合形成膜电极 ,对其电化学性能进行了表征 .
Electrochemical method was used to synthesize doped polypyrrole tungsten-phosphorus-cobalt and tungsten-phosphorus-nickel ternary heteropolyacids. The preparation process is simple and rapid. Two kinds of hybrid organic-inorganic composites are formed on the conductive glassy carbon electrode by electrodeposition , Or directly in polyacid and pyrrole aqueous solution of sulfuric acid to form a membrane electrode, its electrochemical properties were characterized.
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