【摘 要】
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A new polyoxometalate compound formulated as Na2(C3H5N2)4[MnMo9O32]·2H2O 1 has been hydrothermally synthesized and structurally characterized by elemental anal
【机 构】
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Department of Chemistry,Jilin Normal University,Department of Chemistry,Tonghua Teachers College,
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A new polyoxometalate compound formulated as Na2(C3H5N2)4[MnMo9O32]·2H2O 1 has been hydrothermally synthesized and structurally characterized by elemental analysis,IR spectrum and single-crystal X-ray diffraction.The title compound crystallizes in the monoclinic system,space group C2/c,with a = 16.076(2),b = 14.6488(19),c = 18.767(2) ,β = 108.6030(10)o,V = 4188.6(9) 3,C12H24MnMo9N8Na2O34,Mr = 1788.77,Dc = 2.837 g/cm3,μ(MoKα) = 3.024 mm-1,F(000) = 3396,Z = 4,the final R = 0.0270 and wR = 0.0605 for 3829 observed reflections(I > 2σ(I)).
A new polyoxometalate compound formulated as Na2 (C3H5N2) 4 [MnMo9O32] .2H2O 1 has been hydrothermally synthesized synthetically and structurally characterized by elemental analysis, IR spectrum and single-crystal X-ray diffraction. The title compound crystallizes in the monoclinic system, space group C2 = c = 18.767 (2) β, β = 108.6030 (10) o, V = 4188.6 (9) 3, C12H24MnMo9N8Na2O34, Mr = 1788.77, Μ (MoKα) = 3.024 mm-1, F (000) = 3396, Z = 4, the final R = 0.0270 and wR = 0.0605 for 3829 observed reflections (I> 2σ (I)).
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