【摘 要】
：
A new polyoxometalate compound formulated as Na2(C3H5N2)4[MnMo9O32]·2H2O 1 has been hydrothermally synthesized and structurally characterized by elemental anal
【机 构】
：
Department of Chemistry,Jilin Normal University,Department of Chemistry,Tonghua Teachers College,
论文部分内容阅读
A new polyoxometalate compound formulated as Na2(C3H5N2)4[MnMo9O32]·2H2O 1 has been hydrothermally synthesized and structurally characterized by elemental analysis,IR spectrum and single-crystal X-ray diffraction.The title compound crystallizes in the monoclinic system,space group C2/c,with a = 16.076(2),b = 14.6488(19),c = 18.767(2) ,β = 108.6030(10)o,V = 4188.6(9) 3,C12H24MnMo9N8Na2O34,Mr = 1788.77,Dc = 2.837 g/cm3,μ(MoKα) = 3.024 mm-1,F(000) = 3396,Z = 4,the final R = 0.0270 and wR = 0.0605 for 3829 observed reflections(I > 2σ(I)).
A new polyoxometalate compound formulated as Na2 (C3H5N2) 4 [MnMo9O32] .2H2O 1 has been hydrothermally synthesized synthetically and structurally characterized by elemental analysis, IR spectrum and single-crystal X-ray diffraction. The title compound crystallizes in the monoclinic system, space group C2 = c = 18.767 (2) β, β = 108.6030 (10) o, V = 4188.6 (9) 3, C12H24MnMo9N8Na2O34, Mr = 1788.77, Μ (MoKα) = 3.024 mm-1, F (000) = 3396, Z = 4, the final R = 0.0270 and wR = 0.0605 for 3829 observed reflections (I> 2σ (I)).
其他文献
狄更斯(1812——1870)英国著名小说家,出生于海军小职员家庭,10岁时全家被迫迁入负债者监狱,11岁就承担起繁重的家务劳动。曾在皮鞋作坊当学徒,16岁时在律师事务所当缮写员,
天气变得一天比一天冷,我们穿得也一天比一天多起来。而每天都忙于奔波的人们不得不带者手机、BP机、笔记本电脑,以保持与外界的联系、进行商业演示、工作并获取所需要的各种
目的：探讨围手术期患者抗生素合理应用情况及干预措施。方法选取本院收治的128例手术患者，随机将其分为观察组和对照组，各64例，给予对照组患者围术期常规应用抗生素，观察组患者则
为把纪检监察信访举报工作纳入制度化、规范化轨道,不断提高依纪依法做好信访举报工作的水平,根据《中国共产党纪律检查机关控告申诉工作条例》等规定,西藏自治区纪委、监察
一、创设有效教学情境,增加课堂趣味性,激发学生学习兴趣爱因斯坦曾说:“我认为,对一切来说,只有热爱才是最好的教师,它远远超乎责任感。”可见,兴趣在学生的学习活动中起着
Preparation of nanocrystalline 430L stainless steel by both high-energy ball milling and spark plasma sinte- ring technique has been investigated.The results ha
The effects of synthetic Smac peptide(SmacN7) on chemotherapeutic sensitivity of bladder cancer cells were investigated.SmacN7 penetratin peptide was synthesize
下文为慕绥新忏悔录:我深知我的罪行已经给党和人民的事业造成了不可挽回的损失,产生了十分严重的危害。这不仅仅体现在影响沈阳地区的发展和投资环境上,更损害了党在人民心
硫酸钾是一种重要的无氯钾肥，还是一种重要的无机化工原料。我国缺乏天然的硫酸钾资源，国内以各种工艺方法生产的硫酸钾远远不能满足需要，很大一部份需要依赖进口解决。我国已经
近几年来,湖南省资兴市国民经济快速发展, 县域经济综合实力跻身湖南省五强。然而,困难群体的存在和扩大及其生存境遇问题,也凸现在我们面前,成为影响深化改革、推动发展和保