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Three new 2D metal-organic frameworks, [M(BIDPE)2(bdc)2]n(M = Co for 1, Ni for 2) and [Ni(PIDPE)2(H2O)2(bdc)]n(3)(BIDPE = 4,4?-bis(imidazol-1-yl) diphenyl ether, PIDPE =4-(pyridyl)-4?-(imidazol-1-yl) diphenyl ether, bdc2- = 1,3-benzenedicarboxylate), were