【摘 要】
：
The title compound, 2,6-bis(benzimidazo(1,2-c)quinazolin-6-yl)pyridine tetrahy-drate, was synthesized by simple condensation of 2-(2-sminophenyl) benzimidazole
【机 构】
：
College of Chemistry and Materials Science,State Key Laboratory of Structural Chemistry
【基金项目】
：
福建省自然科学基金;the Ministry of Education of China;the Education Department of Fujian Province;the State Key Laboratory of Structural Chemistry
论文部分内容阅读
The title compound, 2,6-bis(benzimidazo(1,2-c)quinazolin-6-yl)pyridine tetrahy-drate, was synthesized by simple condensation of 2-(2-sminophenyl) benzimidazole with pyridine-2,6-dicarboxylic acid and characterized by elemental analysis, IR spectra and single-crystal X-ray diffraction. The crystal belongs to the monoclinic system, space group C2/c with a = 22.226(8), b =16.730(7), c = 16.820(5) (A°),β = 115.796(13)°, V = 5631 (4)(A°)3, C33H27N7O4, Mr= 585.62, Z = 8, Dc= 1.381 g/cm3, λ(MoKa) = 0.71073 (A°), F(000) = 2448 and μ= 0.09 mm-1. The structure was refined to the final R = 0.0730 and wR = 0.1573 for 6346 independent reflections (Rint = 0.0801) and 3384 observed reflections (I> 2σ(I)). In the crystal, the molecules are linked through intermolecular A) are pronounced in the crystal structure.
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