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coordination polymer, [Ni2 (OABDC)(bipy)2(H2O)2]n(H2O)3n (DMBC =5-oxyacetate isophthalic acid) was obtainted by hydrothermal reaction of Ni(NO3)2 and 5-oxyacetate isophthalic acid.In crystal, the centric Ni(Ⅱ) ion was situated in the center a distorted octahedral geometry.