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A binuclear complex including ferrocenyl, Cu2{Fe(C5H5)[C5H4CH2N(CH3)2]}2 (CH3COO)4, was synthesized and characterized by X-ray diffraction. The title complex crystallizes in triclinic, space group P with a = 8.2779(8), b = 9.4830(8), c = 12.262(1) ? = 81.079(5), b = 80.620(4), g = 78.960(4), V = 924.4(1) 3, Z = 1, C34H46Cu2Fe2N2O8, Mr = 849.51, Dc = 1.526 g/cm3, l(MoK) = 0.71073 ? ?= 1.954 mm-1, F(000) = 438, R = 0.0297 and wR = 0.0901. Both cyclopentadienyl rings in each dmaf (dmaf = (dimethylaminomethyl)ferrocene, Fe(C5H5)- [C5H4CH2N(CH3)2]) have an eclipsed conformation. The binuclear molecule has a crystallographic centrosymmetry; four acetates and two Cu atoms form a cage structure with the distance between two neighboring Cu atoms of 2.655(1) .
The title complex crystallizes in triclinic, space group P with a = 8.2779 (A). The title complex crystallizes in triclinic, space group P with a = 8.2779 (8) b = 9.4830 (8) c = 12.262 (1) = 81.079 (5) b = 80.620 (4) g = 78.960 (4) V = 924.4 C34H46Cu2Fe2N2O8, Mr = 849.51, Dc = 1.526 g / cm3, l (MoK) = 0.71073? = 1.954 mm-1, F000 = 438, R = 0.0297 and wR = 0.0901. Both cyclopentadienyl rings in each dmaf (dimethylaminomethyl) ferrocene, Fe (C5H5) - [C5H4CH2N (CH3) 2]) have an eclipsed conformation. The binuclear molecule has a crystallographic centrosymmetry; four acetates and two Cu atoms form a cage structure with the distance between two neighboring Cu atoms of 2.655 (1).