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将恒电流电解在线产生 Cl O-与流动注射化学发光分析法有效地结合 ,基于盐酸阿糖胞苷对 Cl O-- Luminol体系化学发光的拟制作用 ,建立了测定盐酸阿糖胞苷流动注射化学发光新分析法。该法测定盐酸阿糖胞苷的线性范围为 1× 1 0 -8～ 4× 1 0 -7g,检出限为 8× 1 0 -9g,相对标准偏差为 3.0 % ( n=1 1 ) ,已应用于注射用盐酸阿糖胞苷的测定。
Based on the proposed preparation of chemiluminescence of ClO-Luminol by cytarabine hydrochloride, flow cytometry (FCM) was developed for the determination of cytarabine hydrochloride by in-line production of Cl O- by constant current electrolysis and flow injection chemiluminescence analysis. Chemiluminescence new analytical method. The linear range of this method for the determination of cytarabine hydrochloride was 1 × 10 -8 ~ 4 × 10 7 g with a detection limit of 8 × 10 -9 g and a relative standard deviation of 3.0% (n = 11) Has been applied to injection of cytarabine hydrochloride determination.