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This work reports on the production of Ni-50 at% Ti powders by a planetary ball mill in various times(0.5, 1, 2, 6, 20, 36, 54 and 120 h) and subsequent heat treatment in Ar atmosphere at 820 °C. Study of powders structure after milling and heat treatment was carried out by scanning electron microscopy and X-ray diffractometry. According to the results, after milling for 6 hours NiTi phase formed, and by the milling evolution up to 54 h, it became the dominant phase. It was found that by the milling development, a layer structure in powder particles was formed, also by increasing the milling time a more homogeneous structure was obtained. Amorphous Ni Ti transformed into ordered Ni Ti, Ni_3Ti, NiTi_2 and minor TiO_2 and TiO after heat treatment at 820 °C for 1 h.
This work reports on the production of Ni-50 at% Ti powders by a planetary ball mill in various times (0.5, 1, 2, 6, 20, 36, 54 and 120 h) and subsequent heat treatment in Ar atmosphere at 820 ° C. Study of powders structure after milling and heat treatment was carried out by scanning electron microscopy and X-ray diffractometry. According to the results, after milling for 6 hours NiTi phase formed, and by the milling evolution up to 54 h, it became The dominant phase. It was found that by the milling development, a layer structure in powder particles was formed, also by increasing milling time a more homogeneous structure was obtained. Amorphous Ni Ti transformed into ordered Ni Ti, Ni_3Ti, NiTi_2 and minor TiO_2 and TiO after heat treatment at 820 ° C for 1 h.