通过清夜合成法成功地合成了纳米HS沸石，通过 X射线粉末衍射法和高分辨率透射电镜对产物进行了表征，并对其长大机制进行了分析．结果表明，纳米颗粒包含若干个尺寸大致相同而晶体学位向不同的亚晶，其长大机制为聚集增长机制．“,”The nanometer HS zeolite was synthesized from the clear solution methed. The product was charactered by XRD and HRTEM, and the growth mechanism was discussed. The results obtained show that nanoparticles of HS zeolite consist of decades of same-size nanocrystals and the growth mechanism is “growth by aggregation ”