Effect of Sintering Time on Structure and Properties in CuO-doping KNN-LS-BF Piezoelectric Ceramics

来源 :武汉理工大学学报(材料科学版)(英文版) | 被引量 : 0次 | 上传用户:ajing819
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
The 0.6mol% CuO-doping 0.996(0.95Na0.5K0.5NbO3-0.05LiSbO3)-0.004FeBiO3 (KNN-LSBF-CuO) piezoelectric ceramics were synthesized by a solid-state reaction technique, and the structure and piezoelectric properties dependence of sintering time in KNN-LS-BF-CuO ceramics were studied. It is found that all the samples sintered for various time are perovskite structure mixed with orthorhombic symmetry phase and tetragonal phase, but the sintering time has significant influences on the crystalline and properties. When the sintering time increases from 2 hours to 6 hours, the grain of KNN-LS-BF-CuO ceramics becomes more homogeneous and more tight-arrangement. The experimental results reveal that the longer sintering time than 4 hours is beneficial for improving partial properties, such as d33, tgδ, and Qm, but is adverse to εr and kp, the KNNLS-BF-CuO ceramics with optimum properties can be synthesized for 6 hours at 1060 ℃.
其他文献
The dimpling defects caused by conventional hemispherical punch in doubly curved sheet metal reconfigurable die forming process were considered. The rotatable cubic punch (RCP) was developed to suppress the dimpling defects more effectively and convenient
La0.8Sr0.2MnO3 samples with rhombohedral, orthohombic and monoclinic structures were prepared by solid state reaction, sol-gel and co-precipitation methods, respectively. Lattice parameters, grain size, morphology, infrared absorption and emissivity of sa
Catalyst enhanced chemical vapor deposition of nickel film on high Tg polymers such as teflon (PTFE), polyimide(PI), and polysulfone(PS) was investigated by hot wall and cold wall CVD, in which Ni(dmg)2, Ni(acac)2, Ni(hfac)2, Ni(TMHD)2, and Ni(cp)2 are us
Nano-ZrO2 and PEEK particles were synergistically filled in unfilled PTFE to improve the wear resistance and maintain a relatively low friction coefficient, and the materials were studied using a reciprocating sliding friction and wear tester. In the fric
A post-treatment of hydrothermal process was conducted to evaluate its effects on the material characteristics and mechanical properties of plasma-sprayed pure HA and HA/20% YSZ coatings. Surface morphology and microstructural changes, relative element co
The polymeric admixture,the sodium-carboxymethylcellulose (CMC)/poly sodium p-styrene sulfonate (PSS) / poly vinyl acetate (PVAc) was synthesized and applied in cement mortars.The polymer was tested by FTIR and SEM,and the results indicate that the ideal
The nucleation process of graphene films prepared by pulsed laser deposition has been investigated in detail. It is found that graphene nucleates at the steps on the substrate surface firstly, from aggregation of nuclei into particles. High pulsed laser e
In order to explore the effect of high-temperature annealing on the mechanical performances and microstructures of different oxygen SiC fibers, two types of silicon carbide (SiC) -based fibers, specified as XD-SiC fibers (low oxygen) and Nicalon-201 fiber
A recrystallization and partial melting (RAP) process was introduced to prepare the semi-solid 7075 aluminum alloy used for thixoforming. In order to obtain an ideal semi-solid microstructure, a series of extrusion experiments were conducted to comparativ
A plasma cladding experiment was carried out to investigate the characteristics(surface hardness, microstructure, friction, wear properties from different substrates to the cladding layer and the bond strength) of plasma cladding Fe-Cr-Nb-Si-Mo alloy clad