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主要介绍了有机加合物C10H11NO8的合成及结构研究。采用缓慢蒸发溶剂法合成了有机加合物单晶体,该加合物通过红外、热化学和X-射线单晶衍射分析方法确证。X-射线单晶衍射分析显示,晶体中分子主要依靠分子间氢键相互连接,在晶体中构成了氢键网络。对该加合物分子的微观晶体结构进行了讨论。
The synthesis and structure of organic adduct C10H11NO8 are mainly introduced. Single crystals of organic adducts were synthesized using a slow evaporation solvent method and the adducts were confirmed by IR, thermochemistry and single crystal X-ray diffraction analysis. X-ray single crystal diffraction analysis shows that the crystal molecules mainly rely on the intermolecular hydrogen bonds to connect with each other, forming hydrogen bonds in the crystal network. The microscopic crystal structure of the adduct molecule is discussed.