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Depolymerizing polymeric phenylacetylide copper(I)[Cu(C≡CPh)]n with cyclohexyl isocyanide (CNCy) gave the tetranuclear copper(I) complex Cu4(CNCy)4(μ-η^1-C≡CPh)2(μ3-η^1,η^2,η^2C≡CPh)2. The crystal structure was determined X-ray crystallography. The phenyl