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(NH_4)_2MoS_4、FeCl_3与乙二醇钠在乙二醇溶液中反应,再与Bu_4NBr作用可得到一种Mo-Fe-S簇合物[Bu_4N]_3[Mo_2FeS_8O]·HOCH_2CH_2OH,其结构经X光晶体结构分析确定。并测定其红外光谱、紫外光谱、Mossbauer谱和电化学性质。该化合物可催化KBH_4转化乙炔还原为乙烯的反应。
(NH_4) _2MoS_4 and FeCl_3 reacted with sodium ethylene glycol in ethylene glycol solution, and then reacted with Bu_4NBr to obtain a Mo-Fe-S cluster [Bu_4N] _3 [Mo_2FeS_8O] · HOCH_2CH_2OH. Crystal structure analysis confirmed. The infrared spectra, UV spectra, Mossbauer spectra and electrochemical properties were determined. The compound can catalyze the reaction of converting KBH4 to acetylene to ethylene.