最近Svendsen综述了TLC法对不同类型生物碱的分离。对于定量测定植物中托烷和麦角生物碱,TLC法一般是无能为力的,因此,加压-流动平面层析(FFPC)技术的应用是必要的,近年来发展各种分析的FFPC技术,如超压薄层层析(OPLC)和不同类型的旋转平面层析(RPC)。用这两种技术,采用调整操作参数,尤其是使用HPTLC板可以达到高分辨,文中报道了植物中托烷和麦角生物碱的FFPC分离和定量测定。其流动相用“PRISMA”系统优选。它是在不饱和的层析缸中完成的。用甲醇-氯 Svendsen recently reviewed the separation of different types of alkaloids by the TLC method. For the quantitative determination of tropane and ergot alkaloids in plants, the TLC method is generally powerless. Therefore, the application of pressurized-flow planar chromatography (FFPC) technology is necessary. In recent years, various analytical FFPC technologies have been developed, such as super Pressurized layer chromatography (OPLC) and different types of rotational planar chromatography (RPC). Using these two techniques, high resolution can be achieved by adjusting operating parameters, especially using HPTLC plates. FFPC separation and quantitative determination of tropane and ergot alkaloids in plants have been reported. Its mobile phase is optimized using the “PRISMA” system. It is done in unsaturated chromatography tanks. With methanol-chlorine