【摘 要】
：
The title complex Pd(C13H15N2O3)2(C13H15N2O3))- is the anion of isonitrosoethylacetoacetate-N-benzylimine) crystallizes in the monoclinic system, space group P2
【机 构】
：
Central of Laboratory
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The title complex Pd(C13H15N2O3)2(C13H15N2O3))- is the anion of isonitrosoethylacetoacetate-N-benzylimine) crystallizes in the monoclinic system, space group P21/c with a= 8. 197(2), b= 14. 524(3), c= 10. 835(2) A , β= 101.77(3)°, V= 1262. 8(5) A3, Dc=1. 580 g/cm3, F(000)=616, Mr= 600. 94, μ(MoKα) =0. 784mm-1, Z=2 and final R=0. 0410 and wR=0. 0962 for 1855 observed reflections [I≥2σ(I)]. The geometry around the palladium atom is a distorted trans PdN4 square plane, the Schiff base ligand C6H5CH2-IEAI- being coordinated through its oximo-nitrogen atom and imino-nitrogen atom.
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