合成了目标配合物:碘化双 [3,4 二甲氧基苯甲醛缩氨基硫脲]合锌(II),其结构通过单晶X 射线衍射法确定。晶体属单斜晶系,C2/c空间群。配合物分子中,锌(II)与两个硫原子、两个碘原子配位形成轻微畸变的四面体结构,每一个3,4 二甲氧基苯甲醛缩氨基硫脲配体与锌离子处于同一平面内,在晶体中分子之间以氢键连接形成网状结构。 The target complex was synthesized: bis (3,4-dimethoxybenzaldehyde thiosemicarbazone) zinc (II) iodide, the structure of which was determined by single crystal X-ray diffraction. Crystals are monoclinic, C2 / c space group. Complex molecules, zinc (II) and two sulfur atoms, the two iodine atoms form a slightly distorted tetrahedral structure, each 3,4-dimethoxybenzaldehyde thiosemicarbazone ligand and zinc ions in In the same plane, hydrogen bonds are formed between the molecules in the crystal to form a network structure.