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In this paper, we report a simple and facile self-assembly method to successfully fabricate cationic metal porphyrin-MtTMPyP（Mt= Cobalt（Ⅱ）, Manganese（Ⅲ）, or Iron（Ⅲ）; TMPyP = 5, 10, 15, 20-tetrakis（N-methylpyridinium-4-yl） porphyrin） intercalated into the