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The organic-inorganic hybrid polymer [Mn(mbbimb)2(1,5-nds)]n 1 has been synthesized using 1,5-naphthalenedisulfonate (1,5-nds) and 1,3-bis(benzimidazol-1-ylmethyl)- 2,4, 6-trimethylbenzene (mbbimb) with Mn(OAC)2·4H2O in solvothermal reaction. The X-r