建立了生物检材中芬氟拉明的定性定量分析方法。体液及脏器组织经有机溶剂提取后 ,用GC/MS法进行药物筛选、定性 ,生物检材中的芬氟拉明浓度用4 -苯丁胺作内标、GC/NPD法测定。测得芬氟拉明中毒致死者的血液、尿液、肝等组织中浓度分别为7.8μg/ml、64.2μg/ml、31.3μg/g。并对尸体解剖所见及方法可行性进行讨论 The method of qualitative and quantitative analysis of fenfluramine in biological samples was established. Body fluid and visceral tissues were extracted with organic solvents and drug screening was performed by GC / MS. The concentration of fenfluramine in qualitative and biological samples was determined by GC / NPD with 4 - phentermine as internal standard. Measured Fenfluramine intoxication caused by blood, urine, liver and other tissues were 7.8μg / ml, 64.2μg / ml, 31.3μg / g. The body anatomy and methods discussed feasibility