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由酸异丙酯分别与 N,N-双(β-羟乙基)氨基乙酸和酰氯反应共合成了14个新的钛酰基-3-氧代杂氮三环类化合物。进行了元素分析、红外和核磁波谱的测定。首次发现了此类化合物中存在的双分子与水缔合的结构。
A total of 14 novel titanosyl-3-oxa-aza-tricyclic compounds were synthesized by the reaction of acid isopropyl with N, N-bis (β-hydroxyethyl) glycine and acid chloride respectively. Elemental analysis, infrared and nuclear magnetic spectroscopy were performed. For the first time, the bimolecular and water-associated structures found in such compounds were found.