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研究了以愈创木酚为起始原料，经乙酰化、硝化、水解合成５硝基愈创木酚钠的最佳反应条件。以乙酐作酰化剂，１２０℃反应；硝酸加冰乙酸为硝化剂，５０℃硝化；水解在氢氧化钠溶液中进行。５硝基愈创木酚钠收率８６％。
The optimum reaction conditions for the synthesis of 5-nitro guaiacol sodium from guaiacol by acetylation, nitration and hydrolysis were studied. Acetic anhydride as acylating agent, reaction at 120 ℃; nitric acid and acetic acid as nitrating agent, nitration at 50 ℃; hydrolysis in sodium hydroxide solution. 5-nitro guaiacol sodium yield of 86%.