COLORIMETRIC DETECTION OF CARBENICILLIN USING CATIONIC POLYTHIOPHENE DERIVATIVES

来源 :Chinese Journal of Polymer Science | 被引量 : 0次 | 上传用户:yangtt00
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
A water-soluble, polythiophene-based colorimetric sensor was designed for selective and sensitive detection of carbenicillin in HEPES buffer solution. Quaternized quinine was linked to thiophene through bis-functionality benzyl group,which can interact with carbenicillin via electrostatic interaction and geometric match effect. The sensor exhibited a colorimetric signal change upon the addition of carbenicillin because of the formation of more nonplanar structures.However, the addition of other beta-lactam antibiotics or dicarboxylic acids into the sensor solution caused no obvious changes in absorbance intensity ratio. This result may be attributed to the cavity formed by the semi-rigid framework of PTQ2, which is suitable for the special binding with carbenicillin. This novel sensor can effectively distinguish carbenicillin from other beta-lactam antibiotics and has a wide linear range response in HEPES buffer solution. Linear calibration curves are obtained with 0 to 18 μmol/L of HEPES buffer solution, with a limit of detection of 0.54 μmol/L. A water-soluble, polythiophene-based colorimetric sensor was designed for selective and sensitive detection of carbenicillin in HEPES buffer solution. Quaternized quinine was linked to thiophene through bis-functionality benzyl group, which can interact with carbenicillin via electrostatic interaction and geometric match effect. The sensor has a colorimetric signal change upon the addition of carbenicillin because of the formation of more nonplanar structures. Still, the addition of other beta-lactam antibiotics or dicarboxylic acids into the sensor solution caused no significant changes in absorbance intensity ratio. be attributed to the cavity formed by the semi-rigid framework of PTQ2, which is suitable for the special binding with carbenicillin. This novel sensor can effectively distinguish carbenicillin from other beta-lactam antibiotics and has a wide linear range response in HEPES buffer solution. Linear calibration curves are obtained with 0 to 18 μmol / L of H EPES buffer solution, with a limit of detection of 0.54 μmol / L.
其他文献
死亡,与出生和成婚一起,并称为人生的三件大事。中国古代的丧葬礼仪之所以引起研究者的注意,是因为:首先,丧葬礼仪具有强烈的社会意义。人们通过各种丧葬仪式活动不仅要向社会展示
目的:探讨高血脂与年龄、性别和民族的相关性及高血脂与X综合征的关系。方法:采用美国RA-2000型全自动生化分析仪对118例经临床确诊为高血脂,191例血脂正常者进行测定分析。结果:40岁以上的不同年
采用1:3配对病例对照研究方法探讨了痛风致病因素及其相互关系。病例选自近2年内在山东医科大学附属医院确诊的痛风患者26名,每个病例按1:3配比选择对照,要求对照与病例年龄
为了解决站间用明渠及管道连接的半开式梯级串联电站发电系统的水位及频率综合控制问题,提出一种双PID调节器。该调节器对由梯级电站所有机组构成的系统进行联合调节,稳定机
肠道是全身感染的起源,细菌易位在MODS的发生发展中具有重要作用。本实验以放射性同位素35S标记致病Ecoli作示踪剂,研究不同剂量酵母多糖腹腔注射所致MODS时肠道细菌易位的途径和程度,并观察通
2011年,上海通用定下了2015年实现年产销200万辆的目标,并要继续保持在行业中的领先地位。这个蓝图的背景色,是随着中国车市高速发展,越来越多的外资车企涌入,本土品牌也迅速
对比观察活动期SLE患者,正常对照组及SLE患者中西医结合治疗、单纯激素治疗的血浆TXB2、6-K-PGFIα、ⅧR:Ag、血小板聚集等指标的改变,以探讨SLE的瘀血病机及其对治疗的影响。结果表明,SLE患者存在瘀血病机,其
宝马 “BMW之悦” 的品牌宣传活动, 让宝马气质同中国文化有机结合, 推动了客户理解宝马文化内涵, 今年还将延续升级。 面对2012年奥运的到来, 作为中国奥委会官方汽车合作伙伴, “奥运” 也是宝马必然的热词。 如何将这两者更有效的进行结合?  “2012是奥运年, 我们很多市场工作都将围绕奥运这个平台来诠释和传播BMW之悦。 ” 华晨宝马营销高级副总裁戴雷如此解释两者的结合。    数字营销
One new polyoxometalate(POM)-based inorganic–organic hybrid [CdII3(HPO4)(Hbpp)(H2O)2]{CdII[P4-Mo6O28H3.5(OH)3]2}(H4tpb) 7H2O(1)(bpp = 1,3-bis-(4-pyridyl)propan
One of the most common complications of childhood obesity is the non-alcoholic fatty liver disease(NAFLD),which is the most common form of liver disease in chil