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1引言中国药典(二部)1995年版推荐的对乙酰氨基酚(扑热息痛)的测定方法为紫外分光光度法。我们根据其易与Br2发生取代反应的结构特点,采用库仑滴定法以电生溴为滴定剂方法反应速度快,电流效率容易达到100%。用两个极化电极的电流法,即死停终点法指示终点。
1 Introduction Chinese Pharmacopoeia (two) 1995 edition of acetaminophen (paracetamol) determination of UV spectrophotometry. According to its structural characteristics of easy substitution reaction with Br2, the coulometric titration method using electrobrominated bromine as a titrant method has the advantages of fast reaction rate and current efficiency of 100%. The current method with two polarized electrodes, the dead end method indicates the end point.