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The crystal structure of the title compound (C17H19Cl2N2O3P, Mr = 401.21) has been determined by single-crystal X-ray diffraction. The crystal is of monoclinic, space group P21/n with a = 6.1648(6), b = 19.943(2), c = 15.268(2) ?, β = 99.220(2)°, V = 1852.8(3) ?3, Z = 4, Dc = 1.438 g/cm3, F(000) = 832, μ(MoKα) = 0.456 mm-1, the final R = 0.0622 and wR = 0.1586 for 3986 observed reflections (I > 2σ(I)). X-ray analysis reveals that the product is a thermodynamically stable cis isomer. The intramolecular hydrogen bond N(2)–H(2A)…O(1) is observed in the title compound.
The crystal structure of the title compound (C17H19Cl2N2O3P, Mr = 401.21) has been determined by single-crystal X-ray diffraction. The crystal is of monoclinic, space group P21 / n with a = 6.1648 (6), b = 19.943 ), C = 15.268 (2)?,? = 99.220 (2) °, V = 1852.8 (3)? 3, Z = 4, Dc = 1.438 g / cm3, F (000) = 832, 0.456 mm-1, the final R = 0.0622 and wR = 0.1586 for 3986 observed reflections (I> 2σ (I)). X-ray analysis reveals that the product is a thermodynamically stable cis isomer. -H (2A) ... O (1) is observed in the title compound.