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采用间歇玻璃反应釜进行糖精钠与氯甲酸甲酯在丙酮中的缩会反应和N-(2-甲氧甲酰基苯磺酰)氨基甲酸甲酯与2-氨基-4,6-二甲基嘧啶于抽余油中的缩合反应动力学研究。利用序贯实验设计法安排实验点,用Gauss-Newton法进行常微分模型的参数估值,得到了两个反应的动力学方程。
A batch glass reactor was used to carry out the condensation reaction between sodium saccharin and methyl chloroformate in acetone and the reaction of methyl N- (2-methoxycarbonylphenylsulfonyl) carbamate with 2-amino-4,6-dimethyl Study on the Condensation Reaction Kinetics of Pyrimidine in Raffinate Oil. The experimental points were arranged by using the sequential experimental design method and the parameters of the ordinary differential model were estimated by the Gauss-Newton method. The kinetic equations of the two reactions were obtained.