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用双羟基偶氮（或氧化偶氮）苯化合物与对苯二甲酰氯缩聚反应合成了端羟基偶氮（或氧化偶氮）苯低聚物。将其与丁醇醚化氨基树脂进行电场极化交联反应合成交联型非线性光学聚合物。利用红外光谱和紫外可见吸收光谱分别对交联反应、电场极化取向稳定性进行了研究。
Hydroxylazo (or azoxy) benzene oligomers were synthesized by polycondensation of bis-hydroxyazo (or azoxy) benzene with terephthaloyl chloride. Crosslinking reaction was carried out with butanol-etherified amino resin to synthesize the cross-linked non-linear optical polymer. The cross-linking reaction and the polarization stability of the electric field were studied respectively by IR and UV-vis absorption spectra.