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概述了吡虫啉(imidaclaprid)在蔬菜上残留量的测定方法。样品以二氯甲烷为提取剂,氧化铝柱净化,反相高效液相色谱法测定。空白样品添加0003~0009mg的平均回收率为8930%~9567%。最终残留量均低于001mg/kg。降解半衰期21~29天。
The method of determination of residues of imidaclaprid in vegetables is summarized. Samples were extracted with dichloromethane, alumina column purification, determination by reversed-phase high performance liquid chromatography. The average recovery of blank samples from 0003 ~ 0009mg was 8930% ~ 9567%. The final residues were less than 0 01mg / kg. Degradation half-life 2 1 ~ 2 9 days.