Preparation and characterization of neodymium hydroxide powder via the hydration method

来源 :中国化学工程学报(英文版) | 被引量 : 0次 | 上传用户:weiruan007
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The preparation of Nd(OH)3 powder by the direct hydration method using Nd2O3 as a raw material was studied, and the effects of stirring mode, H2O and Nd2O3 molar ratio, stirring rate, and reaction time on temperature change and conversion rate in a hydration system were analyzed. The reasonable process conditions for the direct hydration of Nd(OH)3 by Nd2O3 were then determined. Process, morphology, and structure were considered in the preparation of neodymium hydroxide powder, and its composition was investigated by X-ray powder diffrac-tion, scanning electron microscopy, laser particle size analysis, thermogravimetric differential thermal analysis, and chemical analysis. It has been proved that the process is simple and feasible, in line with the concept of mod- green chemistry, and the products also meet the market requirements.
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