Selective separation and characterization of cyclopeptide alkaloids from Zizyphus jujuba Mill var.sa

来源 :第2届大连国际色谱学术报告会、第37届国际高效液相色谱及相关技术会议、第18届全国色谱学术报告会 | 被引量 : 0次 | 上传用户:zyfblog
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  Cyclopeptide alkaloids in Zizyphus jujuba are important active components which have sedative and hypnotic effects.Due to their low amount, little work on the analysis of cyclopeptide alkaloids has been done.In this paper, the crude extract of Zizyphus jujuba was first analyzed on a Click β-CD column with hydrophilic interaction liquid chromatography (HILIC) method.Cyclopeptide alkaloids were eluted in the first five minutes possibly due to their weak polarities and big ring structures (Fig.1A), while flavonoid glycosides and saponins in Zizyphus jujuba showed good retention under HILIC mode.
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