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采用高效液相色谱法测定秦皮浓缩颗粒中秦皮甲素的含量。色谱柱:Shim-pack CLC-ODS-C18柱);检测波长:254nm;流动相:甲醇-水-冰醋酸(31:69:0.5);流速:1.8mL/min;柱温:40℃;线性关系在0.92~4.60μg范围内,r=0.9996,平均加样回收率为98.42%,RSD为1.70%。
The content of aesculin in Qinpi Concentrate was determined by HPLC. Column: Shim-pack CLC-ODS-C18 column) Detection wavelength: 254 nm Mobile phase: methanol-water-glacial acetic acid (31:69:0.5); Flow rate: 1.8 mL/min; Column temperature: 40 The linear relationship was in the range of 0.92 to 4.60 μg, r=0.9996. The average recovery was 98.42%, and the RSD was 1.70%.