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An organic-inorganic hybrid copper-substituted [Cu(EnMe)2 ]1.5{[Cu(EnMe)2]2-[Cu5Na(OH)4(α-SbW9O33)2]·5.5H2O(I,EnMe = 1,2-diaminopropane) has been hydrothermally synthesized and structurally characterized by elemental analysis,IR spectroscopy and sing