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X射线衍射连续测定相变动力学 R·Ciach等(波-捷) 本文推荐了一种用X射线衍射连续测定相变动力学的方法,将试样和X射线计数管调整在观察衍射线的反射位置,可以连续测定在新相转变时出现的相线强度,计数管可控制其速度。以全部分解的试样为基础,可以预先估计出衍射线的反射位置,同时考虑到应予校正的温度偏差。这种方法所得到的衍射图象是一个连续曲线,表征了新沉淀相
X-Ray Diffraction Continuous Measurement of Phase Transformation Dynamics R · Ciach et al. (Wave-McNair) This paper presents a method for the continuous determination of phase transition kinetics by X-ray diffraction. The sample and X-ray tube are adjusted to observe the reflection position of the diffraction line , You can continuously measure the phase line intensity appears in the new phase transition, counter tube can control its speed. Based on the completely decomposed sample, the reflection position of the diffraction line can be estimated in advance, taking into consideration the temperature deviation to be corrected. The diffraction pattern obtained by this method is a continuous curve characterizing the newly precipitated phase