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本文报道了在D261OCl~-树脂的存在下,仲醇在三相体系中,用次氯酸钙进行氧化,反应在25℃—35℃下进行,生成相应的酮,产率在33—48%之间。
In the presence of D261OCl ~ resin, the secondary alcohol was oxidized with calcium hypochlorite in a three-phase system. The reaction was carried out at 25 ℃ -35 ℃ to yield the corresponding ketone in a yield of 33-48% between.