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设计并组装了一种简易薄层光谱电化学池 .该池具有结构简单、操作方便、对工作电极无透光要求 ,且能适用于多种现场光谱电化学研究的特点 .用该池记录了邻联甲苯胺 高氯酸 醋酸组成的氧化还原体系的荧光光谱电化学和紫外可见光谱电化学响应 ,并用吡啶 氯化钾体系进行了喇曼光谱电化学表征 .
A simple thin-film spectroscopic electrochemical cell was designed and assembled. The cell possessed the characteristics of simple structure, convenient operation, no requirement for working electrode and suitable for many kinds of field-based electrochemical research. O-tolidine perchlorate acetic acid redox system consisting of the redox fluorescence spectroscopy and UV-visible spectroscopy electrochemical response, and the use of pyridine potassium chloride system Raman spectroscopy electrochemical characterization.