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报道了以邻氯苯胺、硫氰酸铵、硫酰氯、亚硝酸钠和氯乙酸乙酯为主要原料合成草除灵乙酯的方法。该工艺总收率为 69 8% ,产品纯度达 98%。
A method for synthesizing selemetylene ethyl ester using o-chloroaniline, ammonium thiocyanate, sulfuryl chloride, sodium nitrite and ethyl chloroacetate as the main raw materials was reported. The total yield of the process was 69.8%, product purity of 98%.