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建立了采用气相色谱-质谱法(GC/MS)确定X胶囊中内容物组成的方法。X胶囊中的内容物研磨成细粉后用乙醚提取,挥干乙醚后,溶于四氢呋喃进样。测定结果表明:样品溶液获得的GC/MS谱图数据与甾体化合物甲基睾丸素(甲睾)非常相似。通过对照发现样品的GC/MS谱图与甲睾标准品的GC/MS谱图完全相同。由此可以鉴定X胶囊样品为甲睾。
A method was established for the determination of the contents of X capsule by gas chromatography-mass spectrometry (GC / MS). X capsule content after grinding into fine powder extracted with ether, evaporated to dryness ether, dissolved in tetrahydrofuran injection. The measurement results show that the GC / MS spectra obtained from the sample solution are very similar to the steroid methyltestosterone (testosterone). The GC / MS spectrum of the sample is exactly the same as the GC / MS spectrum of the testosterone of the testicles. From this it can be identified that the X capsule sample is testosterone.