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报道了 1 ,2 二氢 2 ( 4 氨基苯基 ) 4 [4 ( 4 氨基苯氧基 )苯基 ]( 2H)二氮杂萘 1 酮的合成 ,并用 2D同核化学位移相关谱 ( 1 H ,1 H -COSY) ,2DROESY谱 ,2D异核1 3C - 1 H相关谱和 2D异核1 3C - 1 H多键相关谱 (HMBC)对该化合物的1 H和1 3CNMR谱进行了完整归属 ,证明了此化合物是含二氮杂萘酮结构 ,而不是二氮杂萘醚结构 .
Reported the synthesis of 1, 2 dihydro2 (4-aminophenyl) 4 [4 (4 aminophenoxy) phenyl] (2H) phthalazinone 1 and was characterized by 2D isochrone shift correlation spectroscopy , 1 H -COSY), 2DROESY spectra, 2D heterogeneous 1 3C - 1 H correlation spectra and 2D heterogeneous 1 3C - 1 H multiple bond correlation spectra (HMBC) , It is proved that this compound is a phthalazinone-containing structure instead of the naphthalene ether structure.