通过水热法合成了一个新化合物 [C6 N2 H18]2 [Mo5O15(HPO4 ) 2 ]· H2 O,并通过 IR光谱、ICP、元素分析、差热与热重分析和 X射线单晶衍射分析等手段进行了表征 .结果表明 ,晶体属三方晶系 ,P3 (2 ) 2 1空间群 ,a=1 .1 2 3 1 (1 ) nm,c=2 .2 80 2 (5 ) nm,V=2 .4 91 1 (7) nm3,Dx=2 .83 5 Mg/m3,Z=6,最后的一致性因子 R=0 .0 2 2 7,w R=0 .0 675 .阴离子中 Mo5O15构成一环状结构 ,2个 HPO4 一个连在环的下方 ,一个连在环的上方 ,形成类似于“飞碟”状的结构 ,阳离子为 2个质子化的四甲基乙二胺 A new compound [C6N2H18] 2 [Mo5O15 (HPO4) 2] .H2O was synthesized by hydrothermal method and characterized by IR spectroscopy, ICP, elemental analysis, differential thermal and thermogravimetry and X-ray single crystal diffraction analysis (1) nm, c = 2.802 (5) nm, V = 3.802 (5) nm, 2 .4 91 1 (7) nm3, Dx = 2.83 5 Mg / m3, Z = 6 and the final concordance factor R = 0 .0 2 2 7, w R = 0. A ring structure, two HPO4 connected to the ring one below, one connected to the ring above the formation of similar to the “UFO” -like structure, the cation is two protonated tetramethylethylenediamine