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目的建立开胸顺气胶囊的质量标准。方法采用薄层色谱法对开胸顺气胶囊中的橙皮苷进行定性鉴别,HPLC测定开胸顺气胶囊中氢溴酸槟榔碱的含量。结果定性鉴别结果斑点清晰圆整,分离度好,阴性无干扰,易于鉴别;氢溴酸槟榔碱在81.55~1 957.2μg内线性关系良好(r=1.000),平均回收率为100.6%,RSD为0.88%(n=9)。结论本法可靠、准确、专属性强,可为开胸顺气胶囊的质量控制提供参考。
Objective To establish the quality standard of thoracic cisternal capsule. Methods The hesperidin capsule of thoracotomy was qualitatively identified by TLC. The content of arecoline hydrobromide was determined by HPLC. Results The results of qualitative identification showed that the spots were clear and round, the separation was good and the negative was non-interfering and easy to identify. The iscoline hydrobromide had a good linear relationship (r = 1.000) between 81.55 and 1957.2 μg with an average recovery of 100.6% 0.88% (n = 9). Conclusion This method is reliable, accurate and specific. It can provide a reference for the quality control of Thoracic Gastric Capsule.