,Vibrational modes in La2Zr2O7 pyrochlore irradiated with disparate electrical energy losses

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Polycrystalline samples of La2Zr2O7 pyrochlore are irradiated by different energetic heavy ions to investigate the dependence of the vibrational mode variations on the irradiation parameters.The applied electronic energy loss (dE/dx)e increases from about 5.2 keV/nm to 39.6 keV/nm.The ion fluence ranges from 1 × 1011 ions/cm2 to 6× 1015 ions/cm2.Vibrational modes of irradiated pyrochlore are analyzed by using Raman spectrum.Infrared active modes F1u at 192,308,and 651 cm-1 appear in Raman spectra,and the F2g band at 265 cm-1 rises up due to the irradiation by 200-MeV Kr ions with (dE/dx)e of 16.0 keV/nm.Differently,for the pyrochlore irradiated by 1750-MeV Bi ions with (dE/dx)e of 39.6 keV/nm,in spite of the appearance of infrared active mode F1u 651 cm-1,the amorphous structure occurs according to the vibrational mode variations of pyrochlore irradiated at higher ion fluences.Amorphous tracks are observed in the samples,which confirm the occurrence of pyrochlore-amorphous transition in pyrochlore irradiated with (dE/dx)e of 39.6 keV/nm.
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