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采用电沉积方法,在含KMno4的ZnSO4溶液中,通过控电位和控电流,得到高择优取向的(0002)和(1011)Zn沉积层.用X射线衍射技术和扫描电子显微镜进行表征.结果表明这种高择优取向的Zn沉积层与相应的Zn单晶具有相似的XRD图,且具有比较完整的晶体结构,几乎不存在位错应力;还通过阴极极比曲线讨论了形成高择优取向Zn沉积层的可能原因.
Electrodeposition method was used to obtain highly preferred (0002) and (1011) Zn deposits by potentiostatic and current control in ZnSO4 solution containing KMno4. Characterization by X-ray diffraction and scanning electron microscopy. The results show that the high-oriented Zn deposit has a similar XRD pattern with the corresponding Zn single crystal, and has a relatively complete crystal structure with almost no dislocation stress. The formation of a high preferred orientation Possible Causes of Zn Deposition.