室温离子液体中银纳米微粒的制备与结构表征

来源 :物理化学学报 | 被引量 : 0次 | 上传用户:outopos
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
利用化学还原方法在室温离子液体1-甲基-3-丁基咪唑四氟硼酸盐中制备了金属银纳米微粒,采用X射线衍射,透射电子显微镜,傅立叶红外光谱和热分析对所制备的样品进行了结构表征.结果表明,所制备的银纳米微粒具有立方相结构,粒径约为20nm.离子液体不但作为反应的溶剂而且作为修饰剂修饰在银纳米微粒的表面,从而有效地阻止了银纳米微粒的团聚. Metal silver nanoparticles were prepared by chemical reduction at room temperature in ionic liquid 1-methyl-3-butylimidazolium tetrafluoroborate. The prepared silver nanoparticles were characterized by X-ray diffraction, transmission electron microscopy, Fourier transform infrared spectroscopy and thermal analysis The results show that the prepared silver nanoparticles have a cubic phase with a particle size of about 20nm.Ionic liquid not only acts as a solvent for the reaction but also acts as a modifier on the surface of the silver nanoparticles to effectively prevent Silver nanoparticles agglomeration.
其他文献
11月12~17日,全国政协人口资源环境委员会副主任、国际竹藤组织董事会联合主席、中国花卉协会会长江泽慧率团出席了在新加坡举行的第20届世界兰花大会。
小叶蚊母树(Distyh'umbuxifolium)为金缕梅科蚊母树属常绿灌木,高1~2m,枝叶密集,多分枝,横展生长,嫩枝略有微毛或无毛,顶芽有褐色毛。单叶互生,薄革质,倒披针形,基部狭窄而下延,无毛,全缘,深
师范学校三年制教育是国家教育工作者重要的培养依托,如今却面临着生源与就业的压力,同时也面临着教育对象的特殊性与相应的管理难度。作者作为师范学校三年制的一年级班主任
发展油茶产业,提高农民收入,实现脱贫致富奔小康,具有较大的现实意义和作用。本文介绍了油茶栽培技术,主要包括选择良种壮苗、选地整地、定植、幼林管理、成林管理等内容,笔者结合
The microfabrication and performance NiTi shape memory thin films for microdevice applications were studied by microfabrication processes, which were compatible
Polyetheretherketone (PEEK) based composite materials become of great interest to applications as bearing and slider materials due to their excellent tribologic
This paper deals with the effect of annealing on the magnetism of the sintered NdFeB magnet with a composition of Nd30B5.1Dy1.2A10.6Nb0.7Fe62.4. Microstructural
对于已知波形特征的局部放电信号,选取最优母小波进行多分辨分析,经阈值处理后可以从强干扰中成功地检取出局部放电信息.但对于机理复杂、类型繁多的局部放电而言,单一的最优
Dry machining has become a key issue to significantly reduce the wastes of used lubricants and cleaning agents and to improve the environmental consciousness fo
利用琼斯矩阵理论 ,建立了非保偏光纤光栅环形激光器偏振特性的简化分析模型。通过实验验证 ,利用此模型的分析结果与实验结果是一致的。分析表明 ,采用非保偏光纤制成的激光