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Montmorillonites (MMT) was modified with nonionic surfactant Trion X-100 (OP-10) and anionic surfactants sodium stearate (SSTA) and sodium dodecyl benzene sulfonate (SDBS) respectively.In this study, the effects of anionic surfactant types and MMT types on modification montmorillonite were investigated.XRD analysis results showed that SSTA/OP-10/MMT and SDBS/OP-10/MMT were successfully obtained.