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建立用国产GDX-403固相柱、GC/NPD毛细管气相色谱法,提取、净化生物检材中鸦片的方法。在1ml全血中添加1~4μg混合药物,回收率为79.2%~89.3%,RSD为2.61%~7.50%;在2g肝中添加2.5~10μg混合药物,回收率为72.9%~86.9%,RSD为2.27%~9.20%。该法回收率高,可用于检测人体内的微量鸦片成份。
To establish a domestic GDX-403 solid phase column, GC / NPD capillary gas chromatography, extraction, purification of biological samples of opium method. In 1ml of whole blood, 1 ~ 4μg of mixed drug was added, the recovery was 79.2% ~ 89.3%, RSD was 2.61% ~ 7.50%; 2.5g ~ 10μg mixed drug was added to 2g liver, the recovery was 72 .9% ~ 86.9%, RSD was 2.27% ~ 9.20%. This method has high recovery rate and can be used to detect traces of opium in the human body.