Liquid chromatography coupled with time-of-flight and ion trap mass spectrometry for qualitative ana

来源 :Journal of Pharmaceutical Analysis | 被引量 : 0次 | 上传用户:sxlijx
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
With the expansion of herbal medicine(HM)market,the issue on how to apply up-to- date analytical tools on qualitative analysis of HMs to assure their quality,safety and efficacy has been arousing great attention.Due to its inherent characteristics of accurate mass measurements and multiple stages analysis,the integrated strategy of liquid chromatography(LC)coupled with time-of-flight mass spectrometry(TOF-MS)and ion trap mass spectrometry(IT-MS)is well-suited to be performed as qualitative analysis tool in this field.The purpose of this review is to provide an overview on the potential of this integrated strategy,including the review of general features of LC-IT-MS and LC-TOF-MS,the advantages of their combination,the common procedures for structure elucidation,the potential of LC-hybrid-IT-TOF/MS and also the summary and discussion of the applications of the integrated strategy for HM qualitative analysis(2006-2011).The advantages and future developments of LC coupled with IT and TOF-MS are highlighted. With the expansion of herbal medicine (HM) market, the issue on how to apply up-to- date analytical tools on qualitative analysis of HMs to assure their quality, safety and efficacy has been arousing great attention. Due to its inherent characteristics of accurate mass measurements and multiple stages analysis, the integrated strategy of liquid chromatography (LC) coupled with time-of-flight mass spectrometry (TOF-MS) and ion trap mass spectrometry (IT-MS) is well-suited to be performed as qualitative analysis tool in this field. The purpose of this review is to provide an overview on the potential of this integrated strategy, including the review of general features of LC-IT-MS and LC-TOF-MS, the advantages of their combination, the common procedures for structure elucidation, the potential of LC-hybrid-IT-TOF / MS and also the summary and discussion of the applications of the integrated strategy for HM qualitative analysis (2006-2011). The advantages and future developments of LC coupled with IT and TOF- MS are highlighted.
其他文献
长期以来,初中思想政治课由于受传统教育思想和“应试”倾向的影响,教师心目中的“知识情结”根深蒂固.教师们并不关心自己与学生之间结成的关系,而只关心自己的讲义夹里有多
把维多样性引入粒子群算法并基于混沌变异思想,提出维多样性的动态权重粒子群算法.通过与其它三种不同定权方式的粒子群算法进行比较,证明该方法具有较好的稳定性和有效性,能
在当今社会,科学技术日新月异,经济与信息技术的蓬勃发展,微课作为一种新型的教学模式也日益崛起.微课打破了传统课堂模式,让学生爱上学习,同时也提高了教学质量.把这种新型
一般来讲,生物是一门以综合实验和观察为基本研究方法的实验科学,开展实验教学是高中生物教学过程当中重要的环节.将信息技术应用于高中生物实验教学中,可以有效改善高中生物
该文介绍了一种矩形波导腔多管功率合成器的基本理论,并讨论了四管功率合成器研制结果。该功率合成器作为四管功率合成振荡器用,在单管(耿氏管)额定功率120mW左右时,工作频率
英语素质教育的教学中,优化课堂教学模式是重点,也是实施素质教育的主渠道。要实现优化课堂教学,这就要求我们教师应做到优化教学目标、优化课堂教学的设计、优化教学方法的组合等,通过优化课堂教学模式,以达到实施素质教育的目的。   一、优化教学目标的制订   目标教学是构建素质教育的重点,它要求教师必须了解、熟悉、掌握教学内容,明确教学大纲,要求所要达到的教学目标,通过分层教学,因材施教,使目标教学落
当所有厂商都在推基于Nocona处理器的服务器时,Sun公司再次表现出了他特立独行的一面。8月19日,Sun公司在中国发布了基于Opteron处理器的2路工作站SunJavaWorkstationW2100z
伴随着新课改的不断深入,信息技术在高中生物的教学过程中应用越加广泛.教师需要将信息技术同高中生物的课堂教学有机结合起来,以此有效提升教师的教学效率.教师可以从繁重的
房间隔缺损(ASD)是一种常见的先天性心脏病。经心导管介入治疗继发孔ASD在国内外已广泛开展[1-4],一定程度上替代了心脏直视手术。现对我院行Amplatzer封堵器封堵治疗的ASD患
杜仲浑身是宝 杜仲的皮是名贵的中药材。主治腰膝痛,补中,益精气,坚筋骨,强志,除阴下痒,泾小便,还可治高血压。冠形美丽,果形奇特,夏秋淡绿,深秋褐棕,是良好的庭园观赏树种