以纳米ZnO为催化剂,通过尿素的乙二醇醇解反应合成碳酸乙烯酯,实验表明:在常压下,尿素与干燥的乙二醇比例为1∶1,150℃反应8h,碳酸乙烯酯的产率为90.9%。再以碳酸乙烯酯和芳胺为原料,在Na-Y分子筛和K2CO3催化下,DMF为溶剂,回流反应3h,合成标题化合物,产率50%～85%,并利用元素分析、1HNMR、13CNMR、IR对目标化合物进行了表征。 Nano-ZnO was used as the catalyst to synthesize ethylene carbonate by ethylene glycolysis of urea. The results showed that the ratio of urea to dry ethylene glycol was 1: 1 at 150 ℃ for 8h at atmospheric pressure, and the yield of ethylene carbonate 90.9%. The title compound was synthesized with the yield of 50% ~ 85% by using ethylene carbonate and aromatic amine as raw materials under the catalysis of Na-Y molecular sieve and K2CO3 and DMF as the solvent. After the reaction was refluxed for 3h, the title compound was characterized by elemental analysis, 1HNMR, 13CNMR, The target compounds were characterized by IR.